Analytical Services

The Analytical Services group at New England Discovery Partners (NEDP) provides selected services on a fee-for-service (FFS) basis. At NEDP we understand the time-sensitive nature of analytical data and strive to deliver exceptional service within 24 h of receiving samples.

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY (NMR)

New England Discovery Partners (NEDP) provides one and two-dimensional NMR spectra of common nuclei (1H,13C, 19F and 31P) using Bruker 400 MHz and Bruker 500 MHZ NMR spectrometers. Typical analysis includes the basic spectrum with expansions, integration and peak listing, but a more in-depth analysis with interpretation is also available.

Spectra are provided as pdf documents via e-mail or FAX. A completed sample submission form must be included with all samples. Pricing is based on a per-sample or hourly rate depending on the type of analysis and number of samples.

Pricing

Bruker 400 MHz
1H NMR: $35 / sample (basic analysis)
13C NMR: $65 / sample* (basic analysis)
Hourly Rate: $125 / hour

Bruker 500 MHz
1H NMR : $45 / sample (basic analysis)
13C NMR: $95 / sample (basic analysis)
Hourly Rate: $165 / hour

*assumes sufficient sample for 30 min run time.

Sample Submission Form

The hourly rate includes faxing or E-mailing spectra, sample preparation using our tubes and solvents) and disposing of samples.  Extra solvent charges are included for CD2Cl2, d7-DMF, d8-THF, d6-EtOH.

Optical Rotation

New England Discovery Partners (NEDP) provides optical rotation measurements using a Perkin Elmer PE-341 polarimeter equipped with both Na and Hg source lamps.  As a chemistry CRO, we understand the time-sensitive nature of analytical data and strive to complete all samples within 24 h of receiving them.

Pricing

$50 / Sample

Sample Submission Form

Spectra are provided as pdf documents via e-mail or FAX.  A completed sample submission form must be included with all samples.  Pricing is based on a per-sample basis with discounted rates for larger volumes.

INFRARED AND UV-VISIBLE SPECTROSCOPY

New England Discovery Partners (NEDP) provides Infrared and UV-Visible Spectroscopy measurements using a Thermo-Nicolet 6700 FTIR and Varian Cary 3E UV-Visible Spectrophotometer respectively.  As a chemistry CRO, we understand the time-sensitive nature of analytical data and strive to complete all samples within 24 h of receiving them.

Pricing

Infrared: $48 / Sample

UV-Visible: $42 / Sample

Sample Submission Form

Spectra are provided as pdf documents via e-mail or FAX.  A completed sample submission form must be included with all samples.  Pricing is based on a per-sample basis with discounted rates for larger volumes.

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